Nanoporous Materials through Anodizing of Iron in F-containing Organic Electrolytes

	Nanotech 2011 Vol. 1 Nanotechnology 2011: Advanced Materials, CNTs, Particles, Films and Composites Chapter 4: Nanostructured Coatings, Surfaces & Films
	Nanoporous Materials through Anodizing of Iron in F-containing Organic Electrolytes
Authors:	A. Jagminas, K. Mažeika, V. Klimas
Affilation:	State research institute Center of physical sciences and technology, LT
Pages:	464 - 467
Keywords:	nanoporous films, iron, hematite, synthesis, characterization
Abstract:	In this brief review, our recent progress in fabrication, characterization and application of thick nanoporous iron anodic films in ethylene glycol and a novel dimethyl sulfoxide (DMSO) electrolyte containing some fluorides will be presented and discussed. We have found that DMSO – H2SiF6 process allow fabrication of extremely thick bi-layered films attaining 50 μm and more. Scanning electron microscopy (SEM), X-ray diffraction, Raman, Mössbauer and Furje-transformed IR spectroscopy, and thermo gravimetric analysis (TGA) have been applied here to detect compositional and structural differences of film layers formed at the metal/film interface and at the surface side before and following calcination to hematite
ISBN:	978-1-4398-7142-3
Pages:	882
Hardcopy:	$199.95

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