Nano Science and Technology Institute
Nanotech 2009 Vol. 1
Nanotech 2009 Vol. 1
Nanotechnology 2009: Fabrication, Particles, Characterization, MEMS, Electronics and Photonics
Chapter 4: Nanoscale Characterization

Obtaining and Characterization of Tin Powders by Reactive Milling in Air

Authors:J.O. Lara, A.E.O. Lara, H.B. Ramírez
Affilation:ESIQIE-IPN, MX
Pages:349 - 351
Keywords:nanometric, nodular, morphology, lattice
Abstract:TiN powder was obtained by reactive milling of a titanium powder in air. The Ti powder was milled in an attrition mill. Characterization of the powders was carried out by means of X-ray diffraction (XRD), chemical analysis, and scanning electron microscopy (SEM). The reaction took place in 96 h in the attrition mill. The XRD results indicate that a cubic TiN-like phase crystalline structure was produced in attrition mill, with a lattice parameter of 4.38Å. The morphology of the obtained powders was nodular, with particle size within the nanometric size range.
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