Nano Science and Technology Institute
Nanotech 2008 Vol. 1
Nanotech 2008 Vol. 1
Nanotechnology 2008: Materials, Fabrication, Particles, and Characterization - Technical Proceedings of the 2008 NSTI Nanotechnology Conference and Trade Show, Volume 1
 
Chapter 6: Characterization
 

Synthesis and Characterization of Nanocrystalline Tin Powder by Reactive Milling

Authors:J.O. Lara, H.B. Ramírez
Affilation:Instituto Politécnico Nacional, MX
Pages:955 - 958
Keywords:reactive milling, titanium nitride
Abstract:TiN powder was obtained by reaction milling of a titanium powder in air. The Ti powder was milled in an attrition mill or a Spex mill. Characterization of the powders was carried out by means of chemical analysis, X-ray diffraction (XRD) and scanning electron microscopy (SEM). The reaction took place in 12 h in the Spex mill. It took 96 h in the attrition mill to complete the reaction. The XRD results indicate that a cubic TiN-like phase crystalline structure was produced in the two mills, with a lattice parameter of 4.38 A and 4.23 A, respectively. The morphology of the obtained powders was nodular, with particle size the nanometric size range.
Synthesis and Characterization of Nanocrystalline Tin Powder by Reactive MillingView PDF of paper
ISBN:978-1-4200-8503-7
Pages:1,118
Hardcopy:$159.95
 
Order:Mail/Fax Form
Up
© 2014 Nano Science and Technology Institute. All Rights Reserved.
Terms of Use | Privacy Policy | Contact Us | Site Map